3-HEXENE-2,5-DIONE synthesis
- Product Name:3-HEXENE-2,5-DIONE
- CAS Number:4436-75-3
- Molecular formula:C6H8O2
- Molecular Weight:112.13
625-86-5
210 suppliers
$20.00/25mL
620-02-0
499 suppliers
$14.14/5gm:
4436-75-3
4 suppliers
inquiry
3857-25-8
113 suppliers
$45.00/500 mg
Yield:-
Reaction Conditions:
with oxygen at 50.33; under 7500.75 Torr;Temperature;Pressure;
Steps:
2.2. The thermal oxidation process of DMF
Accelerating rate calorimeter (ARC) (Arthur D. Little Inc. USA, ARC2000) is an excellent thermal analysis instrument to evaluate the thermal stability and safety of hazardous chemicals. It is an attempt that the DMF oxidation process and safety evaluation was measured by ARC, and the measurement conditions are as follows: In the sample container, the shape is spherical bomb, material is titanium, and volume is 8.5 ml. The volume of container plus pipeline is 10 ml. In order to ensure the safety of the experimental process, the sample mass of DMF is 0.2-0.8 g, the initial atmosphere (nitrogen or oxygen) pressure is < 1.0 MPa. The experiment was repeated twice. ARC mode: ‘heat-wait-search’ mode (HWS mode); Start temperature:293.15 K (room temperature);End temperature: 523.15 K;Temperature step: 5.0 K;Temperature sensitivity: 0.01 K; Slope sensitivity: 0.01 K• min -1; pressure sensitivity: 0.1 kPa; Wait time: 20 min;Search time: 10 min.
References:
Huang, Pinxian;Kubota, Shiro;Liu, Pin;Liu, Xiongmin;Saburi, Tei;Wada, Yuji [Thermochimica Acta,2021,vol. 706,art. no. 179078]
625-86-5
210 suppliers
$20.00/25mL
4436-75-3
4 suppliers
inquiry
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
625-86-5
210 suppliers
$20.00/25mL
4436-75-3
4 suppliers
inquiry
131543-46-9
1 suppliers
inquiry
78-98-8
315 suppliers
$10.60/1gm:
15441-67-5
0 suppliers
inquiry
124-38-9
132 suppliers
$175.00/23402
14400-67-0
178 suppliers
$6.00/1g
4436-75-3
4 suppliers
inquiry