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1197371-84-8

3-Hydrazinyl-6-methoxy-2-methylpyridine synthesis

1synthesis methods
52090-56-9 Synthesis
6-Methoxy-2-methylpyridin-3-amine

52090-56-9
130 suppliers
$16.00/250mg

3-Hydrazinyl-6-methoxy-2-methylpyridine

1197371-84-8
9 suppliers
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Yield: 90%

Reaction Conditions:

Stage #1:3-amino-6-methoxy-2-methylpyridine with hydrogenchloride;sodium nitrite in water at 0; for 1.5 h;
Stage #2: with hydrogenchloride;tin(II) chloride dihdyrate in water at 0; for 1 h;

References:

Thomae, David;Jeanty, Matthieu;Coste, Jerome;Guillaumet, Gerald;Suzenet, Franck [European Journal of Organic Chemistry,2013,# 16,p. 3328 - 3336]