3-NITROBENZHYDRAZIDE synthesis
- Product Name:3-NITROBENZHYDRAZIDE
- CAS Number:618-94-0
- Molecular formula:C7H7N3O3
- Molecular Weight:181.15
618-95-1
208 suppliers
$14.00/5g
618-94-0
149 suppliers
$12.00/1mg
Yield:618-94-0 96.2%
Reaction Conditions:
with hydrazine hydrate in ethanol at 85; for 4 h;
Steps:
12 Example 12 3-nitrobenzoylhydrazoneSynthesis
Take a 25ml jar, add 5ml of anhydrous ethanol, 0.53gMethyl 3-nitrobenzoate, stirring, 0.5 g hydrazine hydrate,The reaction was refluxed at 85 °C for 4 h. After the TLC monitoring reaction is over,The ethanol and excess hydrazine hydrate were evaporated under reduced pressure. The silica gel column was separated from the methanol 20:1 by methanol to give an off-white solid of 3-nitrobenzoyl hydrazide 0.51 g.Yield 96.2%.
References:
CN107827776,2018,A Location in patent:Paragraph 0068; 0069; 0070; 0071
121-92-6
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$6.00/25g
618-94-0
149 suppliers
$12.00/1mg
618-98-4
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$13.43/1gm:
618-94-0
149 suppliers
$12.00/1mg
61652-82-2
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618-94-0
149 suppliers
$12.00/1mg
121-90-4
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$24.00/25g
618-94-0
149 suppliers
$12.00/1mg