3-OCTYN-2-OL synthesis
- Product Name:3-OCTYN-2-OL
- CAS Number:41746-22-9
- Molecular formula:C8H14O
- Molecular Weight:126.1962
Yield:41746-22-9 94%
Reaction Conditions:
Stage #1: hex-1-ynewith n-butyllithium in tetrahydrofuran;hexane at -78; for 2.5 h;Inert atmosphere;Schlenk technique;
Stage #2: acetaldehyde in tetrahydrofuran;hexane at -78 - 20; for 18 h;Inert atmosphere;Schlenk technique;
References:
Skotnitzki, Juri;Spessert, Lukas;Knochel, Paul [Angewandte Chemie - International Edition,2019,vol. 58,# 5,p. 1509 - 1514][Angew. Chem.,2019,vol. 131,# 5,p. 1523 - 1527,5] Location in patent:supporting information
15232-76-5
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41746-22-9
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1119-58-0
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2617-03-0
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30503-14-1
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15232-76-5
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41746-22-9
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1119-58-0
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30503-14-1
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802294-64-0
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15232-76-5
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$37.00/1g
41746-22-9
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30503-14-1
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802294-64-0
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109-52-4
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$10.60/1gm:
15232-76-5
50 suppliers
$37.00/1g
41746-22-9
2 suppliers
inquiry
1119-58-0
1 suppliers
inquiry
30503-14-1
0 suppliers
inquiry
109-52-4
352 suppliers
$10.60/1gm: