3-pentan-2-ylphenol synthesis
- Product Name:3-pentan-2-ylphenol
- CAS Number:65392-83-8
- Molecular formula:C11H16O
- Molecular Weight:164.2441
108-95-2
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: copper(l) iodide; 2-Picolinic acid; potassium phosphate / dimethyl sulfoxide / 24 h / 90 °C / Inert atmosphere
2.1: (adamant-1-yl)-acetic acid; potassium carbonate; [RhCl2(p-cymene)]2 / benzene / 24 h / 120 °C / Sealed tube; Inert atmosphere
3.1: methyl trifluoromethanesulfonate / toluene / 2 h / 100 °C / Inert atmosphere
3.2: 0.25 h / Inert atmosphere; Reflux
References:
Li, Gang;Gao, Panpan;Lv, Xulu;Qu, Chen;Yan, Qingkai;Wang, Ya;Yang, Suling;Wang, Junjie [Organic Letters,2017,vol. 19,# 10,p. 2682 - 2685]
97218-43-4
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94-06-4
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$650.00/250mg
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