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77124-20-0

3-PHENOXYCINNAMIC ACID synthesis

14synthesis methods
-

Yield:77124-20-0 94%

Reaction Conditions:

Stage #1: (trimethylsilyl)ketene bis(trimethylsilyl) acetal;3-Phenoxybenzaldehydewith potassium hydroxide in N,N-dimethyl-formamide at 20; for 5 h;
Stage #2: with ammonium chloride in water;

References:

Lensen;Mouelhi;Bellassoued [Synthetic Communications,2001,vol. 31,# 7,p. 1007 - 1011]