3-(thien-2-yl)-1-chloro-propane synthesis
- Product Name:3-(thien-2-yl)-1-chloro-propane
- CAS Number:20906-17-6
- Molecular formula:C7H9ClS
- Molecular Weight:160.6644
Yield:20906-17-6 71%
Reaction Conditions:
Stage #1: thiophenewith n-butyllithium at -50;
Stage #2: 1.3-chlorobromopropane at -78 - 0;
References:
Nair, Sajiv K.;Matthews, Jean J.;Cripps, Stephan J.;Ma, Chunrong;Dovalsantos, Elena Z.;Grubbs, Alan W.;Sach, Neal W.;Hoeve, Wolter ten;Koster, Han;Flahive, Erik J.;Tanis, Steven P.;Renner, Matt;Wiltenburg, Jim van [Tetrahedron Letters,2010,vol. 51,# 11,p. 1451 - 1454] Location in patent:body text
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