3-Thiocyanatopropyltriethoxysilane synthesis
- Product Name:3-Thiocyanatopropyltriethoxysilane
- CAS Number:34708-08-2
- Molecular formula:C10H21NO3SSi
- Molecular Weight:263.43
5089-70-3
314 suppliers
$10.00/5g
333-20-0
414 suppliers
$13.50/100G
34708-08-2
124 suppliers
$21.00/5g
Yield:34708-08-2 92%
Reaction Conditions:
1,8-diazabicyclo[5.4.0]undec-7-ene at 150; for 6 h;
Steps:
1 Application Example 1
106.9g (1.10 mol) potassium thiocyanate, 240.8g (1.00 mol) γ-chloropropyltriethoxysilane, and 0.77g (0.005 mol) 1,8-diazabicyclo[5.4.0]undeca-7-ene (DBU) as a catalyst were placed in a 500-mL four-neck flask equipped with a reflux condenser, a stirrer, and a temperature gauge and subjected to agitation for 6 hours at 150C. Subsequently, reaction by-products were removed by filtering off the reaction product. 242.3g (0.92 mol) of the target ?-thiocyanatopropyltriethoxysilane were isolated by distilling the filtrate under reduced pressure. The yield of the ?-thiocyanatopropyltriethoxysilane was 92%.
References:
EP1428829,2004,A1 Location in patent:Page column 3
5089-70-3
314 suppliers
$10.00/5g
540-72-7
398 suppliers
$13.50/100G
34708-08-2
124 suppliers
$21.00/5g