(5beta,7alpha,12alpha)-7,12-Bis(acetyloxy)-3-oxocholan-24-oic acid synthesis
- Product Name:(5beta,7alpha,12alpha)-7,12-Bis(acetyloxy)-3-oxocholan-24-oic acid
- CAS Number:300386-87-2
- Molecular formula:C28H42O7
- Molecular Weight:490.63
1448-36-8
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300386-87-2
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: 86 percent / TMSOTf / CH2Cl2 / 0.08 h / 20 °C
2: 96 percent / K2CO3; MeOH / 2 h / 20 °C
3: 81 percent / CrO3; aq. H2SO4 / acetone
4: 93 percent / aq. NaOH / propan-2-ol / 80 °C
References:
Opsenica;Pocsfalvi;Juranic;Tinant;Declercq;Kyle;Milhous;Solaja [Journal of Medicinal Chemistry,2000,vol. 43,# 17,p. 3274 - 3282]
4947-65-3
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300386-87-2
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6818-44-6
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300386-87-2
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69889-89-0
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81-25-4
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