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305849-20-1

2,4,6-TriMethyl-N-(4-Methylphenyl)benzenesulfonaMide, 97% synthesis

2synthesis methods
4543-58-2 Synthesis
Benzenesulfonamide, 2,4,6-trimethyl- (9CI)

4543-58-2
46 suppliers
$20.00/1g

1-Butanesulfonic acid, 1,1,2,2,3,3,4,4,4-nonafluoro-, 4-methylphenyl ester

93131-73-8
0 suppliers
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2,4,6-TriMethyl-N-(4-Methylphenyl)benzenesulfonaMide, 97%

305849-20-1
6 suppliers
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Yield:305849-20-1 84%

Reaction Conditions:

with potassium phosphate;tris-(dibenzylideneacetone)dipalladium(0);tert-butyl XPhos in tert-Amyl alcohol at 80; for 16 h;Inert atmosphere;

References:

Shekhar, Shashank;Dunn, Travis B.;Kotecki, Brian J.;Montavon, Donna K.;Cullen, Steven C. [Journal of Organic Chemistry,2011,vol. 76,# 11,p. 4552 - 4563] Location in patent:experimental part