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N-(4-BROMO-2-HYDROXYMETHYL-PHENYL)-4-METHYL-BENZENESULFONAMIDE synthesis

6synthesis methods
5794-88-7 Synthesis
2-Amino-5-bromobenzoic acid

5794-88-7
461 suppliers
$6.00/10g

N-(4-BROMO-2-HYDROXYMETHYL-PHENYL)-4-METHYL-BENZENESULFONAMIDE

329281-02-9
6 suppliers
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
2: pyridine / dichloromethane / 12 h / 0 °C / Inert atmosphere; Reflux

References:

Jia, Min-Qiang;You, Shu-Li [ACS Catalysis,2013,vol. 3,# 4,p. 622 - 624]