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2(1H)-Pyrimidinone, 3,4-dihydro-5-methyl-4-thioxo- (9CI) synthesis

1synthesis methods
-

Yield:35455-79-9 98%

Reaction Conditions:

with diphosphorus pentasulfide;sodium hydrogencarbonate in diethylene glycol dimethyl ether at 110; for 2 h;

References:

Lapucha, Andrzej R. [Synthesis,1987,# 3,p. 256 - 258]