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1-phenyl-2,3,4,9-tetrahydro-1H-beta-carboline hydrochloride synthesis

6synthesis methods
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Yield:3574-01-4 96%

Reaction Conditions:

Stage #1: tryptamine;benzaldehydewith trifluoroacetic acid in 1,2-dichloro-ethane at 110; for 0.0666667 h;Sealed tube;Microwave irradiation;Pictet-Spengler Synthesis;
Stage #2: with hydrogenchloride in ethyl acetate at 20;

References:

Eagon, Scott;Anderson, Marc O. [European Journal of Organic Chemistry,2014,vol. 2014,# 8,p. 1653 - 1665]