[(2-BroMophenyl)Methyl]triphenyl-phosphoniuM BroMide synthesis
- Product Name:[(2-BroMophenyl)Methyl]triphenyl-phosphoniuM BroMide
- CAS Number:36901-75-4
- Molecular formula:C25H21Br2P
- Molecular Weight:512.216
Yield:36901-75-4 99.1%
Reaction Conditions:
in acetone at 20; for 12 h;
Steps:
3.1-2 Synthesis of (2-bromobenzyl)triphenylphosphonium bromide
Multi function cap round bottom 1-bromo-2-(bromomethyl) Benzene to 500 ml (15.0 g, 0.060 mol), Triphenylphosphine (17.316 g, 0.066 mol) gassed up. Herein, as a solvent at room temperature of 63 ml Acetone adaptation stirring time doesn't have any error frames, 12.30.46 g is obtained complete after title compound. (Yield 99.1%).
References:
KR2015/103967,2015,A Location in patent:Paragraph 0111
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