trimethyl-[2-(1,10-phenanthrolin-3-yl)ethynyl]silane synthesis

2synthesis methods

66127-01-3 Synthesis

Yield:369390-65-8 92%

Reaction Conditions:

with copper(l) iodide;triethylamine;bis-triphenylphosphine-palladium(II) chloride in benzene at 80 - 90; for 24 h;Sonogashira coupling;

References:

Schmittel;Michel;Wiegrefe;Kalsani [Synthesis,2001,# 10,p. 1561 - 1567]

66-71-7 Synthesis

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