4-(1-methyl-1H-tetrazol-5-yl)piperidine synthesis
- Product Name:4-(1-methyl-1H-tetrazol-5-yl)piperidine
- CAS Number:1021018-03-0
- Molecular formula:C7H13N5
- Molecular Weight:167.21
1269429-34-6
1 suppliers
inquiry
1021018-03-0
4 suppliers
inquiry
Yield:1021018-03-0 95%
Reaction Conditions:
with hydrogenchloride in 1,4-dioxane at 20; for 1 h;
Steps:
11.B; 12.B
Step B: 4-(l -methyl- lH-tetrazol- 5 -yl)piperidine (i-11); The isomer 1 from Step A above (45 mg, 0.16 mmol) was dissolved in 4 M HC1 in dioxane (1.0 mL) and stirred at RT for 1 h. The product was concentrated under reduced pressure and dried under high vacuum to give the title compound (i-l 1) (25 mg, 95%). ESI-MS calculated for T-I^Ns: Exact Mass: 167.13; Found 168.12.
References:
WO2012/12314,2012,A1 Location in patent:Page/Page column 55
1401728-91-3
7 suppliers
inquiry
1021018-03-0
4 suppliers
inquiry
91419-58-8
5 suppliers
inquiry
1021018-03-0
4 suppliers
inquiry
280111-63-9
4 suppliers
inquiry
1021018-03-0
4 suppliers
inquiry
10315-07-8
136 suppliers
$10.00/250mg
1021018-03-0
4 suppliers
inquiry