4-(2-aminoethyl)-2,6-diiodo-phenol synthesis
- Product Name:4-(2-aminoethyl)-2,6-diiodo-phenol
- CAS Number:370-00-3
- Molecular formula:C8H9I2NO
- Molecular Weight:388.97
788824-51-1
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Yield:370-00-3 100%
Reaction Conditions:
with hydrogenchloride in ethyl acetate at 20; for 3 h;
Steps:
Synthetic procedure for 3,5-diiodo-tyramine (compound C)
Compound A (1000 mg), HCl 37% (1 mL) and EtOAc (3 mL) were placed into a round bottom flask equipped with a magnetic stirring bar. The mixture was stirred at room temperature for 3 h. The crude reaction mixture was evaporated under reduced pressure and the residue was neutralized with 10% NaHCO3 and filtered affording white solids in a quantitative cleavage. 1H NMR (600 MHz, DMSO-d6) δ 7.64 (s, 2H, H-2), 2.97 (t, 2H, H-6), 2.76 (t, 2H, H-5).
References:
Restrepo, Manuel Pastrana;Surmay, Verónica Surmay;Jaramillo, Elkin Galeano;Restrepo, Sara Robledo [Journal of the Brazilian Chemical Society,2019,vol. 30,# 1,p. 116 - 123]
51-67-2
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64318-28-1
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