4-(2-Cyanophenyl)benzonitrile synthesis
- Product Name:4-(2-Cyanophenyl)benzonitrile
- CAS Number:42289-52-1
- Molecular formula:C14H8N2
- Molecular Weight:204.23
Yield:42289-52-1 98 %Chromat.
Reaction Conditions:
Stage #1: o-cyanobromobenzenewith n-butyllithium in tetrahydrofuran;hexane at 24; for 1.63889E-05 h;Flow reactor;
Stage #2: with Trimethyl borate in tetrahydrofuran;hexane at 24; for 0.000555556 h;Flow reactor;
Stage #3: 4-iodobenzonitrile in tetrahydrofuran;methanol;hexane at 120; for 0.156667 h;Flow reactor;Suzuki-Miyaura Coupling;Temperature;
References:
Nagaki;Hirose;Moriwaki;Mitamura;Matsukawa;Ishizuka;Yoshida [Catalysis science and technology,2016,vol. 6,# 13,p. 4690 - 4694]
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