4,4-Dihexyl-4H-cyclopenta[1,2-b:5,4-b']dithiophene synthesis
- Product Name:4,4-Dihexyl-4H-cyclopenta[1,2-b:5,4-b']dithiophene
- CAS Number:153312-86-8
- Molecular formula:C21H30S2
- Molecular Weight:346.59
51751-44-1
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$7.00/100mg
153312-86-8
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Schlenk technique; Inert atmosphere
1.2: 3 h / -78 - 0 °C / Schlenk technique; Inert atmosphere
2.1: potassium hydroxide; hydrazine hydrate / ethylene glycol / 2 h / 200 °C / Inert atmosphere
3.1: potassium hydroxide; potassium iodide / dimethyl sulfoxide / 12 h / 0 - 20 °C / Inert atmosphere
References:
Aghazada, Sadig;Gao, Peng;Yella, Aswani;Marotta, Gabriele;Moehl, Thomas;Teuscher, Joël;Moser, Jacques-E.;De Angelis, Filippo;Grätzel, Michael;Nazeeruddin, Mohammad Khaja [Inorganic Chemistry,2016,vol. 55,# 13,p. 6653 - 6659]
![3,4-Dithia-7H-cyclopenta[a]pentalene](/CAS/GIF/389-58-2.gif)
389-58-2
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$24.00/100mg
111-25-1
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$10.00/5g
153312-86-8
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389-58-2
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$24.00/100mg
544-10-5
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$13.00/5g
153312-86-8
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![4H-Cyclopenta[2,1-b:3,4-b']dithiophen-4-one](/CAS/GIF/25796-77-4.gif)
25796-77-4
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$22.00/100mg
153312-86-8
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498-62-4
412 suppliers
$5.00/1g
153312-86-8
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