4,4'-dimethyldiphenyliodonium synthesis
- Product Name:4,4'-dimethyldiphenyliodonium
- CAS Number:6293-68-1
- Molecular formula:
- Molecular Weight:0
624-31-7
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Yield:6293-68-1 99.7%
Reaction Conditions:
with ammonium persulfate in sulfuric acid;toluene;
Steps:
4 EXAMPLE 4
EXAMPLE 4 To a mixture of p-iodotoluene (10.85 parts) and toluene (18.4 parts) in 83.5 parts of a 73.5% by weight aqueous sulfuric acid was 20.5 parts of ammonium persulfate. The resulting mixture was treated in the same way as in Example 1. There was obtained 20.5 parts of di(p-tolyl)iodonium bromide (yield 99.7%).
References:
US4659840,1987,A
108-88-3
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