4-(4-METHYL-BENZYL)-PIPERIDINE synthesis
- Product Name:4-(4-METHYL-BENZYL)-PIPERIDINE
- CAS Number:92822-01-0
- Molecular formula:C13H19N
- Molecular Weight:189.3
872-85-5
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 75 min, 2.) THF, hexane, from -78 deg C to -20 deg C, 2 h
2: 11.2 g / H2, conc. HCl / 20 percent Pd/C / methanol / 16 h
References:
Wright, Jon L.;Gregory, Tracy F.;Bigge, Christopher F.;Boxer, Peter A.;Serpa, Kevin;Meltzer, Leonard T.;Wise, Lawrence D.;Cai, Sui Xiong;Hawkinson, Jon E.;Konkoy, Christopher S.;Whittemore, Edward R.;Woodward, Richard M.;Zhou, Zhang-Lin [Journal of Medicinal Chemistry,1999,vol. 42,# 13,p. 2469 - 2477]
![Piperidine, 4-[(4-methylphenyl)methylene]-1-(phenylmethyl)-](/CAS/20210305/GIF/242487-87-2.gif)
242487-87-2
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92822-01-0
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33974-28-6
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106-38-7
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3762-25-2
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