4-(5-METHYL-1,2,4-OXADIAZOL-3-YL)BENZOYL CHLORIDE synthesis
- Product Name:4-(5-METHYL-1,2,4-OXADIAZOL-3-YL)BENZOYL CHLORIDE
- CAS Number:222541-76-6
- Molecular formula:C10H7ClN2O2
- Molecular Weight:222.63
95124-68-8
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222541-76-6
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Yield:222541-76-6 100%
Reaction Conditions:
Stage #1: 4-(5-methyl-1,2,4-oxadiazol-3-yl)benzoic acidwith N,N-dimethyl-formamide in dichloromethane at 0; for 0.0833333 h;
Stage #2: with oxalyl dichloride in dichloromethane at 25; for 4 h;
References:
Xiong, Wenzhang;Shi, Qiu;Liu, Wenbo H. [Journal of the American Chemical Society,2022,vol. 144,# 34,p. 15894 - 15902] Location in patent:supporting information