4-Amino-3-methoxybenzamide synthesis
- Product Name:4-Amino-3-methoxybenzamide
- CAS Number:211374-82-2
- Molecular formula:C8H10N2O2
- Molecular Weight:166.18
92241-87-7
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Yield:211374-82-2 100%
Reaction Conditions:
with hydrogen;palladium 10% on activated carbon in ethanol at 20; for 19 h;
Steps:
1b.2
The title compound 14B 500 mg, 2.55 mmol), 10% palladium on carbon (100 mg), and ethanol (50 ml) were stirred at room temperature under a hydrogen atmosphere for 19 hours. The reaction was then filtered through celite and the filtrate evaporated under reduced pressure to give the title compound as a beige solid. (450 mg, 2.7 mmol, >100%). LCMS: [M+H]+=167, Rt = 0.54 min, 70% purity.
References:
WO2007/59905,2007,A2 Location in patent:Page/Page column 43
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211374-82-2
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5081-36-7
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211374-82-2
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