4-CHLORO-4'-ETHYLBENZOPHENONE synthesis
- Product Name:4-CHLORO-4'-ETHYLBENZOPHENONE
- CAS Number:71766-56-8
- Molecular formula:C15H13ClO
- Molecular Weight:244.72
637-87-6
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63139-21-9
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13007-92-6
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$41.70/1g
71766-56-8
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$294.00/1g
Yield:71766-56-8 95%
Reaction Conditions:
with sodium t-butanolate in N,N-dimethyl acetamide at 80; for 0.25 h;Suzuki Coupling;
Steps:
2.6 Typical Procedure for the Carbonylative Suzuki Coupling Reaction in the Presence of SBA-16/DFMP-Pd
General procedure: Aryl halide (1.0 mmol), arylboronic acid (1.1 mmol),t-BuONa (2.0 mmol), SBA-16/DFMP-Pd (0.0026 g,0.2 mol%), and Cr(CO)6 (0.5 mmol, 0.11 g) in DMA(3.0mL) was stirred in a flask at 80°C. The reaction progress was monitored by thin layer chromatography (TLC).Upon the reaction’s completion, the mixture was allowed to cool down to room temperature and then filtered and washed with H2Oand ethyl acetate. The organic fraction was separated,dried over anhydrous Na2SO4 and then the solvent was removed using a rotary evaporator. Further purification was performed on silica gel column chromatography to afford the pure products.
References:
Niakan, Mahsa;Asadi, Zahra;Emami, Mohammad [Catalysis Letters,2020,vol. 150,# 2,p. 404 - 418]
63139-21-9
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$5.00/250mg
122-01-0
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$13.00/25g
71766-56-8
20 suppliers
$294.00/1g
637-87-6
302 suppliers
$38.00/10g
63139-21-9
290 suppliers
$5.00/250mg
199620-15-0
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71766-56-8
20 suppliers
$294.00/1g
100-41-4
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122-01-0
380 suppliers
$13.00/25g
71766-56-8
20 suppliers
$294.00/1g