ChemicalBook CAS DataBase List 4-CHLOROBENZENEDIAZONIUM HEXAFLUOROPHOSPHATE

4-CHLOROBENZENEDIAZONIUM HEXAFLUOROPHOSPHATE synthesis

1synthesis methods

Product Name:4-CHLOROBENZENEDIAZONIUM HEXAFLUOROPHOSPHATE
CAS Number:1582-27-0
Molecular formula:C6H4ClF6N2P
Molecular Weight:284.53

106-47-8 Synthesis

106-47-8
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4-CHLOROBENZENEDIAZONIUM HEXAFLUOROPHOSPHATE

1582-27-0
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Yield:1582-27-0 58%

Reaction Conditions:

Stage #1: 4-chloro-anilinewith hydrogen hexafluorophosphate (V) in water monomer at 20; for 0.0333333 h;Inert atmosphere;
Stage #2: with NaNO₂ in water monomer at 0; for 0.25 h;Inert atmosphere;

References:

Akram, Manjur O.;Mali, Pramod S.;Patil, Nitin T. [Organic Letters,2017,vol. 19,# 12,p. 3075 - 3078] Location in patent:supporting information

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