4-CHLOROPHENYL BENZOATE synthesis
- Product Name:4-CHLOROPHENYL BENZOATE
- CAS Number:2005-08-5
- Molecular formula:C13H9ClO2
- Molecular Weight:232.66
55-21-0
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Yield: 71%
Reaction Conditions:
with iron(III) nitrate hexahydrate;trifluorormethanesulfonic acid in o-xylene at 80;
Steps:
9 Synthesis of p-chlorophenyl benzoate
In a reaction tube containing 70 mol% of Fe (NO3) 3 · 6H20 catalyst, 0.2 mmol of benzamide, 20 mol% of trifluoromethanesulfonic acid, 2 ml Solvent 1,2-xylene, 0.2mmo 1 p-chlorophenol, reacted at 80 ° C. After the reaction, the mixture was washed with water or a saturated salt solution, extracted with chloroform, dried and concentrated under reduced pressure to remove the solvent. Chromatographic separation gave the target product: 71% yield.
References:
Hubei College Of Sciences And Technology;Chen Xiuling;Sun Shaofa;Wu Minghu;Wang Jian;Guo Haibing;Li Yan CN106831285, 2017, A Location in patent:Paragraph 0051-0053
591-50-4
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2005-08-5
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100-52-7
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2005-08-5
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2005-08-5
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