4-Cyclooctene-1-carboxylic acid synthesis
- Product Name:4-Cyclooctene-1-carboxylic acid
- CAS Number:4103-10-0
- Molecular formula:C9H14O2
- Molecular Weight:154.21
Yield:4103-10-0 65%
Reaction Conditions:
Stage #1: 5-bromocyclooct-1-enewith iodine;magnesium in tetrahydrofuran;Reflux;Grignard Reaction;
Stage #2: carbon dioxide in tetrahydrofuran; for 48 h;Grignard Reaction;
References:
Bell, Craig A.;Blinco, James P.;Ediriweera, Gayathri R.;Fletcher, Nicholas L.;Fuchs, Adrian V.;Houston, Zachary H.;Howard, Christopher B.;Mahler, Stephen M.;Simpson, Joshua D.;Thurecht, Kristofer J.;Van De Walle, Matthias;Venkatachalam, Taracad K. [Chemical Science,2020,vol. 11,# 12,p. 3268 - 3280]
111-78-4
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4103-10-0
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124-38-9
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4103-10-0
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