4-ethynyl-2-Methylpyridine synthesis
- Product Name:4-ethynyl-2-Methylpyridine
- CAS Number:30413-56-0
- Molecular formula:C8H7N
- Molecular Weight:117.15
761426-51-1
9 suppliers
inquiry
30413-56-0
35 suppliers
$90.00/250mg
Yield:30413-56-0 88%
Reaction Conditions:
with potassium carbonate in methanol at 60; for 2 h;
Steps:
203
A suspension of 2-methyl-4-[(trimethylsilyl)ethynyl]pyridine (1.63 g, 8.62 mmol) and potassium carbonate (5.95 g, 43.1 mmol) in methanol (30 mL) was stirred for 2 h at 60 0C. The methanol was evaporated in vacuo, water was added and the mixture was extracted with dichloromethane. The combined organic phases were dried over sodium sulfate and
References:
WO2008/76046,2008,A1 Location in patent:Page/Page column 188-189
22282-99-1
397 suppliers
$6.00/5g
1066-54-2
475 suppliers
$9.00/10g
30413-56-0
35 suppliers
$90.00/250mg
22282-99-1
397 suppliers
$6.00/5g
30413-56-0
35 suppliers
$90.00/250mg