4-IODOANILINE HYDROCHLORIDE synthesis
- Product Name:4-IODOANILINE HYDROCHLORIDE
- CAS Number:74367-81-0
- Molecular formula:C6H7ClIN
- Molecular Weight:255.48
636-98-6
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Yield:74367-81-0 86%
Reaction Conditions:
Stage #1: p-nitrobenzene iodidewith iododioxobis(triphenylphosphine)rhenium(V);Dimethylphenylsilane in toluene; for 1.5 h;Reflux;
Stage #2: with hydrogenchloride in diethyl ether;toluene;
References:
De Noronha, Rita G.;Romao, Carlos C.;Fernandes, Ana C. [Journal of Organic Chemistry,2009,vol. 74,# 18,p. 6960 - 6964] Location in patent:supporting information; experimental part
540-37-4
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106-50-3
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