(4'-METHOXYBIPHENYL-3-YL)-METHANOL synthesis
- Product Name:(4'-METHOXYBIPHENYL-3-YL)-METHANOL
- CAS Number:20854-56-2
- Molecular formula:C14H14O2
- Molecular Weight:214.26
Yield:20854-56-2 495 mg
Reaction Conditions:
Stage #1: 3-iodobenzylalcoholwith dmap;polystyrene siloxane resin;triethylamine in dichloromethane at 20; for 1 h;
Stage #2: 4-methoxyphenylboronic acidwith potassium carbonate;palladium diacetate in 1,4-dioxane;water at 100; for 15 h;Suzuki coupling;
References:
Meloni, Marco M.;White, Peter D.;Armour, Duncan;Brown, Richard C.D. [Tetrahedron,2007,vol. 63,# 2,p. 299 - 311]
57455-06-8
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