4-Methoxypiperidine synthesis
- Product Name:4-Methoxypiperidine
- CAS Number:4045-24-3
- Molecular formula:C6H13NO
- Molecular Weight:115.17
553672-12-1
4045-24-3
The general procedure for the synthesis of 4-methoxypiperidine from the compound (CAS: 553672-12-1) was as follows: the compound (620 mg) obtained in step (1) was dissolved in methanol (20 mL) and 10% palladium-carbon catalyst (80 mg) was added. The reaction mixture was stirred for 3 hours at room temperature and under hydrogen atmosphere. Upon completion of the reaction, the reaction mixture was filtered through a membrane filter and the filtrate was concentrated under vacuum to afford 4-methoxypiperidine (290 mg, yield: 100%) as a light yellow oil. Mass spectrometry analysis (APCI) showed m/z: 116 [M + H]+.
553672-12-1
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4045-24-3
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Yield:4045-24-3 100%
Reaction Conditions:
with hydrogen;palladium 10% on activated carbon in methanol at 20; for 3 h;
Steps:
10.2
To a solution of the compound obtained in the above step (1) (620 mg) in methanol (20 mL) was added 10 % palladium-carbon (80 mg) and the mixture was EPO
References:
TANABE SEIYAKU CO., LTD. WO2007/46550, 2007, A1 Location in patent:Page/Page column 116-117
141047-49-6
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4045-24-3
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620-08-6
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4045-24-3
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4045-25-4
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$7.00/250mg
4045-24-3
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188622-27-7
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4045-24-3
149 suppliers
$38.00/1g