(4-METHYL-PIPERAZIN-1-YL)-ACETIC ACID synthesis
- Product Name:(4-METHYL-PIPERAZIN-1-YL)-ACETIC ACID
- CAS Number:54699-92-2
- Molecular formula:C7H14N2O2
- Molecular Weight:158.2
60-29-7
0 suppliers
$30.00/50g
54699-92-2
130 suppliers
$8.00/250mg
Yield: 90%
Reaction Conditions:
in 1-acetoxy-2-(4-methyl-piperazino)-ethane;water
Steps:
3 Example 3
Example 3 Preparation of (4-methylpiperazinyl) acetic acid (VII) A 22 g solution of (4-methylpiperaziny) ethyl acetate (VI) in 500 ml of water was stirred at the reflux temperature of the solvent for 2 h. The reaction mixture was evaporated to dryness, thus obtaining a residue which, by grinding with a 8:2 diethylether/acetone mixture, provided 16.75 g (yield 90%) of a white solid with a melting point of 160-2 °C, identified as (4-methylpiperazinyl) acetic acid (VII).
References:
LABORATORIOS RUBIO, S.A. EP693481, 1996, A1
28920-67-4
36 suppliers
$55.00/250mg
54699-92-2
130 suppliers
$8.00/250mg
835916-40-0
0 suppliers
inquiry
54699-92-2
130 suppliers
$8.00/250mg
5780-70-1
42 suppliers
$151.58/1g
54699-92-2
130 suppliers
$8.00/250mg
109-01-3
678 suppliers
$5.00/5 g
96-34-4
356 suppliers
$10.00/25g
54699-92-2
130 suppliers
$8.00/250mg