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4-NAPHTHALEN-1-YL-MORPHOLINE synthesis

14synthesis methods
-

Yield:98223-72-4 99%

Reaction Conditions:

with bis(1,5-cyclooctadiene)nickel (0);lithium tert-butoxide;1,3-bis[2,6-bis(1-methylethyl)phenyl]-1,3-dihydro-2H-imidazol-2-ylidene monohydrochloride in 1,4-dioxane at 100; for 12 h;Schlenk technique;Inert atmosphere;

References:

Li, Jing;Wang, Zhong-Xia [Organic Letters,2017,vol. 19,# 14,p. 3723 - 3726] Location in patent:supporting information