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36884-75-0

4-Pentenal, 5-phenyl-, (4E)- synthesis

5synthesis methods
4393-06-0 Synthesis
3-Phenylpropene-3-ol

4393-06-0
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4-Pentenal, 5-phenyl-, (4E)-

36884-75-0
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-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: mercury(II) acetate / Ambient temperature
2: 31 percent Spectr. / methylaluminum bis(4-bromo-2,6-di-tert-butylphenoxide) (reagent A) / CH2Cl2 / 0.25 h / -78 °C

References:

Nonshita, Katsumasa;Banno, Hiroshi;Maruoka, Keiji;Yamamoto, Hishashi [Journal of the American Chemical Society,1990,vol. 112,# 1,p. 316 - 322]