2-Pyridinecarboxylicacid,1,6-dihydro-5-methyl-6-oxo-,methylester(9CI) synthesis
- Product Name:2-Pyridinecarboxylicacid,1,6-dihydro-5-methyl-6-oxo-,methylester(9CI)
- CAS Number:401792-80-1
- Molecular formula:C8H9NO3
- Molecular Weight:167.16
401792-77-6
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401792-80-1
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Yield:401792-80-1 60%
Reaction Conditions:
Stage #1: methyl 5-methyl-2-pyridinecarboxylate N-oxidewith acetic anhydride for 3 h;Heating;
Stage #2: with sodium methylate in methanol at 0; for 0.166667 h;
References:
Adamczyk, Maciej;Akireddy, Srinivasa Rao;Reddy, Rajarathnam E. [Tetrahedron Asymmetry,2001,vol. 12,# 17,p. 2385 - 2387]
589-93-5
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$33.78/5ML
401792-80-1
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29681-38-7
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$13.00/100mg
401792-80-1
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4434-13-3
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$21.00/250mg
401792-80-1
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