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ChemicalBook CAS DataBase List 2-(2-Oxopropyl)-7-hydroxy-5-methyl-4H-1-benzopyran-4-one
40738-40-7

2-(2-Oxopropyl)-7-hydroxy-5-methyl-4H-1-benzopyran-4-one synthesis

10synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: potassium carbonate / acetone / 5 h / Reflux
2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 20 h / 20 °C
3: sodium hydride / tetrahydrofuran / 3.5 h / Inert atmosphere; Reflux
4: boron tribromide / dichloromethane / 18 h / 20 °C

References:

Liu, Qingyin;Mu, Yu;An, Qi;Xun, Jiali;Ma, Jian;Wu, Wenxi;Xu, Minjuan;Xu, Jun;Han, Li;Huang, Xueshi [Bioorganic Chemistry,2020,vol. 94,art. no. 103420]