
1-O-Methyl-3,5-bis-O-[(2,4-dichlorophenyl)methyl]-alpha-D-erthro-pentofuranoside-2-ulose synthesis
- Product Name:1-O-Methyl-3,5-bis-O-[(2,4-dichlorophenyl)methyl]-alpha-D-erthro-pentofuranoside-2-ulose
- CAS Number:443642-30-6
- Molecular formula:C20H18Cl4O5
- Molecular Weight:480.17

168427-35-8
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$45.00/250mg
![1-O-Methyl-3,5-bis-O-[(2,4-dichlorophenyl)methyl]-alpha-D-erthro-pentofuranoside-2-ulose](/CAS/GIF/443642-30-6.gif)
443642-30-6
52 suppliers
$75.00/50mg
Yield:443642-30-6 90%
Reaction Conditions:
Stage #1: (3R,4S,5R)-4-((2,4-dichlorobenzyl)oxy)-5-(((2,4-dichlorobenzyl)oxy)methyl)-2-methoxytetrahydrofuran-3-olwith trichloroisocyanuric acid in dichloromethane at 0; for 0.166667 h;Inert atmosphere;
Stage #2: with 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical in dichloromethane at 20; for 3 h;Inert atmosphere;
References:
Zeng, Debin;Zhang, Rui;Nie, Quandeng;Cao, Lin;Shang, Luqing;Yin, Zheng [ACS Medicinal Chemistry Letters,2016,vol. 7,# 12,p. 1197 - 1201] Location in patent:supporting information

677299-16-0
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![1-O-Methyl-3,5-bis-O-[(2,4-dichlorophenyl)methyl]-alpha-D-erthro-pentofuranoside-2-ulose](/CAS/GIF/443642-30-6.gif)
443642-30-6
52 suppliers
$75.00/50mg

168427-36-9
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![1-O-Methyl-3,5-bis-O-[(2,4-dichlorophenyl)methyl]-alpha-D-erthro-pentofuranoside-2-ulose](/CAS/GIF/443642-30-6.gif)
443642-30-6
52 suppliers
$75.00/50mg