5-(2-NITROPHENYL)THIOPHENE-2-CARBALDEHYDE synthesis
2synthesis methods
- Product Name:5-(2-NITROPHENYL)THIOPHENE-2-CARBALDEHYDE
- CAS Number:42545-34-6
- Molecular formula:C11H7NO3S
- Molecular Weight:233.24
Yield:42545-34-6 68%
Reaction Conditions:
with 1,10-Phenanthroline;di-tert-butyl peroxide;oxygen;potassium carbonate;copper(I) bromide in toluene at 140; for 24.25 h;Molecular sieve;Schlenk technique;Sealed tube;regioselective reaction;
References:
Patra, Tuhin;Nandi, Sudip;Sahoo, Santosh K.;Maiti, Debabrata [Chemical Communications,2016,vol. 52,# 7,p. 1432 - 1435] Location in patent:supporting information
