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890007-17-7

5-(3-methoxyphenyl)-1H-pyrazole-3-carbohydrazide synthesis

2synthesis methods
5-(3-methoxyphenyl)-1H-pyrazole-3-carbohydrazide

890007-17-7
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: sodium ethanolate / ethanol / 7 h / 0 - 20 °C
2: hydrazine hydrate; acetic acid / 0 °C / Reflux
3: hydrazine hydrate / ethanol / 36 h / Reflux

References:

Wu, Deyan;Jin, Fangfang;Lu, Weiqiang;Zhu, Jin;Li, Cui;Wang, Wei;Tang, Yun;Jiang, Hualiang;Huang, Jin;Liu, Guixia;Li, Jian [Chemical Biology and Drug Design,2012,vol. 79,# 6,p. 897 - 906]