5-BROMO-2-IODO-M-XYLENE synthesis
- Product Name:5-BROMO-2-IODO-M-XYLENE
- CAS Number:206559-43-5
- Molecular formula:C8H8BrI
- Molecular Weight:310.96
24596-19-8
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$8.00/10g
206559-43-5
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$10.00/1g
Yield:206559-43-5 96%
Reaction Conditions:
with hydrogenchloride;potassium iodide;sodium nitrite in water;acetonitrile at 0;
Steps:
1 4-bromo-2,6-dimethyliodobenzene]
In 0 ° C in acetonitrile with sodium nitrite and hydrochloric acid 4-bromo-2,6-dimethylanilinewas diazotized, by converting theamino group to iodine by the addition of potassium iodide, 4-bromo-2,6-dimethyliodobenzene was obtained in 96% yield.This method is a known method of the literature (NonPatentDocument 2) describes.
References:
Nagoya University;Kaneka Corporation;Yamaguchi, Shigehiro;Wakamiya, Atsushi JP5959171, 2016, B2 Location in patent:Paragraph 0258-0260
87-62-7
464 suppliers
$10.00/5 g
206559-43-5
132 suppliers
$10.00/1g