1-Bromo-4-iodobenzene synthesis
- Product Name:1-Bromo-4-iodobenzene
- CAS Number:589-87-7
- Molecular formula:C6H4BrI
- Molecular Weight:282.9
673-40-5
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589-87-7
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Yield:589-87-7 99%
Reaction Conditions:
with potassium iodide in water at 25; for 0.0833333 h;Sandmeyer Reaction;Solvent;
Steps:
3.2. General Procedure for Synthesis of Aryl Iodides (2)from Aryl Diazofluoroborates
General procedure: To a suspension of aryl diazofluoroborate (1 mmol) inwater (3mL), aqueous solution of potassium iodide (1.5 mmol in 2mL H2O) was added in single lot at room temperature.Reaction mixture was stirred for specific time (Table 2).The solid product was separated by filtration and the liquidproducts were separated by extraction in diethyl ether (5mL).The organic layer was dried over anhydrous Na2SO4 andsolvent was removed at room temperature afforded pure iodocompounds in excellent yields. Further all synthesized compoundswere characterized and confirmed by comparisonwith reported aryl iodides.
References:
Gholap, Somnath S. [Letters in Organic Chemistry,2018,vol. 15,# 7,p. 594 - 599]
106-40-1
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589-87-7
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5467-74-3
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589-87-7
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540-37-4
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589-87-7
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108-86-1
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$10.00/5g
589-87-7
541 suppliers
$10.00/1g