5-CHLORO-6-NITROQUINOLINE synthesis
- Product Name:5-CHLORO-6-NITROQUINOLINE
- CAS Number:58416-32-3
- Molecular formula:C9H5ClN2O2
- Molecular Weight:208.6
712-33-4
17 suppliers
inquiry
56-81-5
1771 suppliers
$5.00/25g
58416-32-3
10 suppliers
inquiry
58416-31-2
25 suppliers
inquiry
Yield:58416-32-3 48% ，58416-31-2 22%
Reaction Conditions:
Stage #1: 3-chloro-4-nitroacetanilide;glycerolwith sulfuric acid;4-chloro-aniline for 3 h;Reflux;Skraup-Doebner-Von Miller reaction;
Stage #2: with ammonia in water;
References:
Lan, Tian;Yuan, Xian Xia;Yu, Jiang Hong;Jia, Chao;Wang, Yu Shi;Zhang, Hui Juan;Ma, Zi Feng;Ye, Wei Dong [Chinese Chemical Letters,2011,vol. 22,# 3,p. 253 - 255] Location in patent:experimental part
825-41-2
152 suppliers
$6.00/1g
56-81-5
1771 suppliers
$5.00/25g
58416-32-3
10 suppliers
inquiry
58416-31-2
25 suppliers
inquiry
712-33-4
17 suppliers
inquiry
58416-32-3
10 suppliers
inquiry
588-07-8
107 suppliers
$22.19/25g
58416-32-3
10 suppliers
inquiry
108-42-9
476 suppliers
$10.00/5g
58416-32-3
10 suppliers
inquiry