5-FLUORO-2-METHOXYCINNAMIC ACID synthesis
- Product Name:5-FLUORO-2-METHOXYCINNAMIC ACID
- CAS Number:157518-45-1
- Molecular formula:C10H9FO3
- Molecular Weight:196.18
459-60-9
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$7.00/5g
157518-45-1
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$42.79/250mg
Yield:-
Steps:
Multi-step reaction with 3 steps
1: conc. HCl, conc. H2SO4 / 3 h / 70 °C
2: 54 percent / hexamethylenetetramine, aq. HOAc / 2 h / Heating
3: 96.6 percent / piperidine / pyridine / 1) room temperature, 16 h; 2) 60 deg C, 4 h; 3) 100 deg C, 3 h
References:
Vallaerda, Jerk;Appelberg, Ulf;Csoeregh, Ingeborg;Hacksell, Uli [Journal of the Chemical Society. Perkin transactions I,1994,# 4,p. 461 - 470]
141-82-2
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$5.00/25g
19415-51-1
178 suppliers
$8.00/1g
157518-45-1
38 suppliers
$42.79/250mg
19415-40-8
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inquiry
157518-45-1
38 suppliers
$42.79/250mg
19415-51-1
178 suppliers
$8.00/1g
157518-45-1
38 suppliers
$42.79/250mg