5-Formyl-2-methylbenzoic acid synthesis
- Product Name:5-Formyl-2-methylbenzoic acid
- CAS Number:105650-34-8
- Molecular formula:C9H8O3
- Molecular Weight:164.16
68120-35-4
75 suppliers
$15.00/250mg
105650-34-8
39 suppliers
$45.00/2.5g
Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C
1.2: 0.17 h
2.1: methanesulfonic acid / 3 h / 0 - 65 °C
3.1: Dess-Martin periodane / dichloromethane / 1.17 h / 0 - 20 °C
4.1: water; sodium hydroxide / ethanol; tetrahydrofuran
References:
BOEHRINGER INGELHEIM INTERNATIONAL GMBH;MADANAHALLI RANGANATH RAO, Jagannath;GURRAM RANGA, Madhavan;PACHIYAPPAN, Shanmugam WO2014/202528, 2014, A1
72985-21-8
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inquiry
105650-34-8
39 suppliers
$45.00/2.5g
675148-96-6
37 suppliers
$80.00/250mg
105650-34-8
39 suppliers
$45.00/2.5g
104-87-0
526 suppliers
$6.00/25g
105650-34-8
39 suppliers
$45.00/2.5g
36276-24-1
129 suppliers
$31.00/1g
105650-34-8
39 suppliers
$45.00/2.5g