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5-nitro-2,3-dihydro-1H-inden-1-one synthesis

8synthesis methods
Benzaldehyde, 2-ethenyl-4-nitro-

1313762-43-4
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Yield:22246-24-8 93%

Reaction Conditions:

with bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate;6-diphenylphosphinomethyl-3-methyl-2-aminopyridine in toluene at 150; for 1 h;Inert atmosphere;

References:

Vautravers, Nicolas R.;Regent, Damien D.;Breit, Bernhard [Chemical Communications,2011,vol. 47,# 23,p. 6635 - 6637] Location in patent:supporting information; experimental part