5-phenylfuran-2-boronic ester synthesis
- Product Name:5-phenylfuran-2-boronic ester
- CAS Number:1396752-91-2
- Molecular formula:C16H19BO3
- Molecular Weight:270.13
17113-33-6
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Yield:1396752-91-2 28%
Reaction Conditions:
Stage #1: 2-phenylfuranwith n-butyllithium in tetrahydrofuran at -78; for 0.5 h;
Stage #2: 2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane in tetrahydrofuran at -78 - 20;
References:
Rabal, Obdulia;José-Enériz, Edurne San;Agirre, Xabier;Sánchez-Arias, Juan Antonio;Vilas-Zornoza, Amaia;Ugarte, Ana;De Miguel, Irene;Miranda, Estíbaliz;Garate, Leire;Fraga, Mario;Santamarina, Pablo;Perez, Raul Fernandez;Ordo?ez, Raquel;Sáez, Elena;Roa, Sergio;García-Barchino, María José;Martínez-Climent, José Angel;Liu, Yingying;Wu, Wei;Xu, Musheng;Prosper, Felipe;Oyarzabal, Julen [Journal of Medicinal Chemistry,2018,vol. 61,# 15,p. 6518 - 6545]
108-86-1
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