5-Phenyltetrahydrofuran-2-ol synthesis
- Product Name:5-Phenyltetrahydrofuran-2-ol
- CAS Number:36866-66-7
- Molecular formula:C10H12O2
- Molecular Weight:164.2
1008-76-0
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$58.00/5g
36866-66-7
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Yield:36866-66-7 96%
Reaction Conditions:
Stage #1: 4,5-dihydro-5-phenyl-2(3H)-furanonewith polymethylhydrosiloxane;(η(5)-C5H5)2Ti(OC6H4Cl-p)2;tetrabutylammonium fluoride on alumina in toluene at 20;hydrosilylation;
Stage #2: with sodium hydroxide in tetrahydrofuran;toluene at 20; for 1 h;desilylation;
References:
Verdaguer, Xavier;Hansen, Marcus C.;Berk, Scott C.;Buchwald, Stephen L. [Journal of Organic Chemistry,1997,vol. 62,# 24,p. 8522 - 8528]
638-37-9
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591-51-5
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$123.00/50ml
2085-90-7
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36866-66-7
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29021-82-7
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36866-66-7
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100-52-7
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$20.37/250g
36866-66-7
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