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Trisilane, 2-bromo-1,1,1,3,3,3-hexamethyl-2-(trimethylsilyl)- synthesis

12synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: potassium tert-butylate / tetrahydrofuran / 4 h / 20 °C / Schlenk technique
2: ethylene dibromide / toluene / 0 - 20 °C / Schlenk technique

References:

Iwamoto, Takeaki;Nukazawa, Takumi;Sasaki, Hayato;Yokouchi, Yuki [Organometallics,2021,vol. 40,# 15,p. 2415 - 2419]