5H-Benzocyclohepten-5-one, 6,7,8,9-tetrahydro-6-methyl- synthesis

8synthesis methods

67-56-1 Synthesis

Yield:51490-09-6 94%

Reaction Conditions:

with trimethylamine-N-oxide;tricarbonyl(η⁴-1,3-bis(trimethylsilyl)-4,5,6,7-tetrahydro-2H-inden-2-one)iron;potassium tert-butylate at 110; for 24 h;

References:

Polidano, Kurt;Allen, Benjamin D. W.;Williams, Jonathan M. J.;Morrill, Louis C. [ACS Catalysis,2018,vol. 8,# 7,p. 6440 - 6445]

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