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ChemicalBook CAS DataBase List ethyl 4-aMino-1-benzyl-5-oxo-2,5-dihydro-1H-pyrrole-3-carboxylate
53720-95-9

ethyl 4-aMino-1-benzyl-5-oxo-2,5-dihydro-1H-pyrrole-3-carboxylate synthesis

3synthesis methods
-

Yield:53720-95-9 364 mg

Reaction Conditions:

with ammonium formate in ethanol at 78; for 24 h;

Steps:

4.2 Step 2

Compound 2 (366 mg, 1.4 mmol) and ammonium formate (176 mg, 2.81 mmol) were added to ethanol (2 mL), and then stirred at 78 °C for 24 h. After the reaction, it was spin-dried, and the residue was crystallized from ethanol to obtain compound 3 (364 mg)

References:

CN113683616,2021,A Location in patent:Paragraph 0223-0227; 0229